Dissolving Palladium in Hydrochloric acid and Clorox?

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dbrick81

Member
Joined
Dec 29, 2007
Messages
17
Location
Delaware
Will Hydrochloric acid and Clorox dissolve palladium well enough to test some monolithic capacitors with stannous chloride. If it will, should I first dissolve base metals with Acid peroxide.

Thanks
 
Brick,

I have not tested HCl-Cl with Palladium, but it should work. I have dissolved Pd with AP several times. It is very slow, but it works.

I cover this process in depth on the upcoming PGM DVD soon to be released.

Crush and grind the caps in a mortar and pedstal or ball mill before you begin. Wear a dusk mask as the ceramic is Barium based and is easily airborne when grinding!! [img:33:25]http://www.goldrecovery.us/images/skullnbones_smallrev.jpg[/img]

The best method of stripping the base metals from the monolithic capacitiors is to use straight HCl. I let them soak for four hours in the first HCl wash and then overnight in a second HCl wash then I move on to processing for the Palladium. Heating the HCl will speed this process.

The first wash typically produces a purple liquid (tin/nickel/lead) . The second wash turns out pale lime green (nickel).[img:33:25]http://www.goldrecovery.us/images/skullnbones_smallrev.jpg[/img]


Steve
 

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