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Gently boyl for 2 hours with AR .
Solution should have a reddish hue.
Add spare ammount of NH4Cl.
The reddish hue gets stonger.
Apply heat. When hot enough pore
the clear solution to a 2nd glass. When
it gets cold you should view yellow/
orange precipitate
 
Try adding a sample to Ar and heat. Then add a few drops of Stannous chloride. If it's in there and leachable you will get a positive reaction.
 
PGM ores tend to be very complex with the values dispersed in a matrix of silicates and Aluminates with Iron oxides and sometimes alloyed with iron or Nickel. The best prep is to grind it to a fine powder. Sometimes it helps to digest the pulp in Sodium peroxide or Sodium Hydroxide to a red heat before you try to digest in AR. Fine particles trapped in the matrix can't be digested until they are exposed for chemical attack.

Extract the residue in dilute HCl and digest in AR.
 
is finding the PGMs. The hard part is figuring a way to economically extract the values without polluting the environment or killing yourself.
 

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