There is an analytical procedure used to analyze gold cyanide plating solutions which essentially drops out the gold which you weigh for the analytical result. This is usually done with 5 ml samples of plating solution so you would need to evaporate down the solution you have to a concentrate of about 50 ml. The procedure requires acidification of a cyanide solution which is always done in a good laboratory hood, which is why I asked.
As you are working in the back yard, neighbors or not, I do not feel it is safe for you to employ the method I am considering, so in the interest of your safety I respectfully decline to detail the procedure.
As you are working in the back yard, neighbors or not, I do not feel it is safe for you to employ the method I am considering, so in the interest of your safety I respectfully decline to detail the procedure.