wmhunter86
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- Joined
- Jul 8, 2019
- Messages
- 7
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I understand it is hard to refine so I'm prepared to get less than if the metals were individual.Its kinda hard to find a comp on that one: 35Pd, 30Ag, 14Cu, 10Au, 10Pt, 1Zn.
I would have an interest in purchasing it but I’m going to be cheap on it. It is a pain to refine so expect a haircut whatever you do with it.
With only 1% base metals this alloy should not be that difficult to refine for someone with pgm experience. Or am i missing something?I understand it is hard to refine so I'm prepared to get less than if the metals were individual.
Besides the copper? The part that makes it a pain is its right in the special zone that everything wants to drag something else along with it.With only 1% base metals this alloy should not be that difficult to refine for someone with pgm experience. Or am i missing something?
Yep, leave a seat for me.you are right, copper is a base metal too. I did't think it was troublesome with pgm's.
Obviously i do not have enough pgm experience. Sorry, I'll quietly go back to my corner.
I would like to see if this can be treated in nitric as is... Just from curiosity. It would be slow and you will need to go with more than 35% nitric, but I will say this should lead to some workable solution of Ag+Pd+Cu+Zn+some Pt, and solid AuPt+some undissolved Pd residue. Soilds can be then dissolved in AR or other chloride media and gold dropped in reasonable purity, leaving PGMs behind. Tougher part would be to sharply separate Ag from Pd without trapping Pd in AgCl for example. But this can be done relatively well, despite washing the AgCl can take some time and effort.Its kinda hard to find a comp on that one: 35Pd, 30Ag, 14Cu, 10Au, 10Pt, 1Zn.
I would have an interest in purchasing it but I’m going to be cheap on it. It is a pain to refine so expect a haircut whatever you do with it.
I would think that conc nitric would pretty much dissolve everything into solution. Anyone who tries to refine this material i hope has a good understanding of platinosis and safety precautions.As much as drag down may (or not) be an issue the real issue is all the different steps you would need to go through to get full separation of all the different metals - with 30 percent silver just for starters you would likey need to start with inquarting - then etc. etc. etc. (sorry on my phone so hard to post details) Kurt.
The issue is that if there is Pd/Pt alloy the Pd will drag the Pt with it into solution.I believe that Pd is the only PGM that dissolves in Nitric Acid and I seem to recall that even that is not complete. The wire would probably have to be inquarted to get a good separation of the other PGMs from the Silver/Pd and base metals.
I believe that Pd is the only PGM that dissolves in Nitric Acid and I seem to recall that even that is not complete.
Note the bold print of + some Pt being dissolve with the nitricIt would be slow and you will need to go with more than 35% nitric, but I will say this should lead to some workable solution of Ag+Pd+Cu+Zn+some Pt,
In other words - with this alloy (as is) HOT nitric will dissolve the silver & Pd along with likely at least some Pt - leaving the gold & some Pt undissolved & possibly a trace of Pd undissolved due to the Au & Pt in the alloy --- however - you should be able to get all the Pd to go into solution if you run the reaction at a simmer/boil & for prolonged time to insure all the Pd dissolvesand solid AuPt+some undissolved Pd residue
Besides the copper?
I weighed it today and it is 86 grams. I would sell it to a reputable refinery/buyer but have had a hard time finding one of those. I am open to any suggestions the members have on a person/business they suggest as a reputable refinery/buyer.
I still have it. Willing to let it go for $1300.I have been out for a bit. Do you still have your material or did you get it to move along?
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