Pirotechnia
Member
- Joined
- Jul 24, 2011
- Messages
- 8
Hi all,
I am new to this forum. I am very much into old fashion assay, crucible method and scorification but have not very much experience about cupellation. Although I have studied the process in great detail from books, both new and old ones. In this google books is a true treasure, which I strongly recommend (you are probably already well aware about).
First question:
I wonder if anyone of you have heard of a custom of involving multiple cupellations of gold?
I mean, this after the parting phase.
As I have understood it, one will recieve collect 99.5% pure gold after the first parting so I cannot really see any point of doing this. However, I am curious to know if you have heard about it or if there is such a custom at all.
Second question:
I am a bit confused about the proportions of lead / bismuth, some books mention this as being of great importance while others seem to say that it's not important at all! I have for example read that about 10 parts of lead is being used in relation to the gold per se (not counting the addition of inquartation i.e. 3 parts of silver).
Third question:
I have read in "A manual of pratical assay" by John Mitchell, that its possible to make direct cupellation of silver bearing
galena per se or by the addition of 2 parts of lead. Is this something which anyone in here have tried? Or direct (without roasting) cupellation of other minerals as for example pyrites containing gold.
Fourth question:
I read in an old book that one should perform a cupellation assay with such a minor proportions as 11 grains of lead, 2 (or 3) grains of silver and 1 grain of gold. This seem very weard to me, because as far as I am concerned one grain represents only 0.006 gram! Any ideas? I am well aware that the weight systems have changed a lot since the last couple of hundred years and is very different in different nations, but the term "grain" is derived from the latin "granum" and should not be that easy to confuse. Any input is welcome.
Thanks in advance!
/Pirotechnia
P.S. I am about to set up a fire assay lab during this autumn, consider to buy my self a small Cress furnace or a Vcella (6), which seems to be the best alternatives after some research in this forum and in other places.
I am new to this forum. I am very much into old fashion assay, crucible method and scorification but have not very much experience about cupellation. Although I have studied the process in great detail from books, both new and old ones. In this google books is a true treasure, which I strongly recommend (you are probably already well aware about).
First question:
I wonder if anyone of you have heard of a custom of involving multiple cupellations of gold?
I mean, this after the parting phase.
As I have understood it, one will recieve collect 99.5% pure gold after the first parting so I cannot really see any point of doing this. However, I am curious to know if you have heard about it or if there is such a custom at all.
Second question:
I am a bit confused about the proportions of lead / bismuth, some books mention this as being of great importance while others seem to say that it's not important at all! I have for example read that about 10 parts of lead is being used in relation to the gold per se (not counting the addition of inquartation i.e. 3 parts of silver).
Third question:
I have read in "A manual of pratical assay" by John Mitchell, that its possible to make direct cupellation of silver bearing
galena per se or by the addition of 2 parts of lead. Is this something which anyone in here have tried? Or direct (without roasting) cupellation of other minerals as for example pyrites containing gold.
Fourth question:
I read in an old book that one should perform a cupellation assay with such a minor proportions as 11 grains of lead, 2 (or 3) grains of silver and 1 grain of gold. This seem very weard to me, because as far as I am concerned one grain represents only 0.006 gram! Any ideas? I am well aware that the weight systems have changed a lot since the last couple of hundred years and is very different in different nations, but the term "grain" is derived from the latin "granum" and should not be that easy to confuse. Any input is welcome.
Thanks in advance!
/Pirotechnia
P.S. I am about to set up a fire assay lab during this autumn, consider to buy my self a small Cress furnace or a Vcella (6), which seems to be the best alternatives after some research in this forum and in other places.