Refining gold powder in hydrochloric acid and hydrogen peroxide

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Rreyes097

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So I tried to refine some of my gold powder with hydrochloric acid and hydrogen peroxide 3%. I read that that was okay to use for refining. But I couldn't find a solid answer on how to precipitate it. Either copper or smb? I felt copper wouldn't be helping clean it purify the gold so I used smb. The good dropped but it's very fine particles and doesn't want to settle so I'm not sure this was a great idea. I read that this process was good for refining but the gold the way it is now isn't going to be easy to clean and wash and rinse. Did I do something wrong? Was I simply wrong to use this process for purifing gold in the first place? I tried researching this but only found examples of people accidentally dissolving their gold in AP. Then they would cement with copper.
 
So I tried to refine some of my gold powder with hydrochloric acid and hydrogen peroxide 3%. I read that that was okay to use for refining. But I couldn't find a solid answer on how to precipitate it. Either copper or smb? I felt copper wouldn't be helping clean it purify the gold so I used smb. The good dropped but it's very fine particles and doesn't want to settle so I'm not sure this was a great idea. I read that this process was good for refining but the gold the way it is now isn't going to be easy to clean and wash and rinse. Did I do something wrong? Was I simply wrong to use this process for purifing gold in the first place? I tried researching this but only found examples of people accidentally dissolving their gold in AP. Then they would cement with copper.
You can dissolve Gold by HCl and Peroxide, but you need much higher strength around 20-30 % I'd guess.
Precipitation as normal.
Very fine particles hints to low concentration, so I'd guess you diluted it too much during addition on too low concentration Peroxide.
 

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