Goldenchild is exactly right when he says to add nitric acid literally by the drop.
You will be amazed at how little nitric it takes when you are dissolving foils.
Early on in my education here I learned of and started using Harold's method of putting a small button of gold in my beaker to use up excess nitric. When I first started doing that I found I was dissolving as much as 1/2 gram of gold to kill the nitric.
I switched to using an eyedropper to add nitric, and using medium heat on my hotplate. If all activity stops and you have just a bit of gold left to dissolve, add one drop and wait a few minutes. Repeat this process until your gold is dissolved and you won't have any problem getting it to precipitate.
Using the proper amount of nitric is much better and less time consuming than trying to kill the excess.
You will be amazed at how little nitric it takes when you are dissolving foils.
Early on in my education here I learned of and started using Harold's method of putting a small button of gold in my beaker to use up excess nitric. When I first started doing that I found I was dissolving as much as 1/2 gram of gold to kill the nitric.
I switched to using an eyedropper to add nitric, and using medium heat on my hotplate. If all activity stops and you have just a bit of gold left to dissolve, add one drop and wait a few minutes. Repeat this process until your gold is dissolved and you won't have any problem getting it to precipitate.
Using the proper amount of nitric is much better and less time consuming than trying to kill the excess.