Hi! This forum has been an invaluable (thank you!) resource as I slog through the final stages of processing this auriferous....quartz-pebble conglomerate?...paleoplacer?...thing. Photos to follow.
-I used the following process to arrive originally at a homogenous +-55% Au concentrate from about 91lbs of the pictured material
1. used a heavy duty barrel tumbler to ball mill 2-3in pieces to a thin slurry containing a lot of small quartz pebbles and a bunch of fine gold
2. strained and allowed whatever passed a (sorry, I can't find a number on it to be precise with mesh but it's blue, traps sand, and fits on a 5 gallon bucket if that helps ID it) fine sieve to settle out, then pouring off
**At this stage I took a sample from 15 lbs of a uniform powder I recovered from steps 1&2 which tested very consistently both as a powder and a bead -- but was determined to be out of the refiner's wheelhouse in that form.
"Enough Au content by far, but it would have to be melted into a solid." Unfortunately, the combination of my gravely limited grasp of smelting/flux/what-the-heck-I'm-even-doing and even more limited propane melting furnace has -- you guessed it-- limited my ability to make the jump from concentrate to metallic gold with that many impurities present. In an effort to avoid doing an AR process, (time constraints but also...I'm leery of turning gold I can see into gold I can't in a process I've done successfully before -- but I suspect mainly from luck) I scoured the forums for anything relevant. Did those things. I arrived at a powder that appears to meet all the physical criteria for a much higher purity Au by:
3. following the instructions for rinsing the mud in Hcl/Ammonia/water cycles found here on the forum + diluted sodium nitrate solution at one point for kicks
4. used stove and pyrex 9x13 to dry the mud in batches (though I do think it behaves more like cornstarch/water will when you try to manipulate it - which was cool, and surprised me)
4. Repeat.
There was a lot of free gold in the material, and any grit was easily snagged by the sieve, not to mention the filters; otherwise I would feel truly silly claiming these approx. values. That being said, I estimate I will end up with 35 or so lbs (18lbs currently processed with the additional cleaning steps) of a powder that, with a confirmed Au content of at least 55% should theoretically be easy to smelt for someone with the experience and equipment to do it properly. If you are that person and would like to speak about a really favorable trade for your services, please message me! Regarding the photos of the final result - I could not get a photo that showed the true color for some reason, but it is very much the pale cinnamon I have seen described here. Any glitter would be a residual Pyrex sliver from a near-catastrophic lesson in the limits of bakeware as labware that occasionally crop up and are removed. Thank you!
Andi
-I used the following process to arrive originally at a homogenous +-55% Au concentrate from about 91lbs of the pictured material
1. used a heavy duty barrel tumbler to ball mill 2-3in pieces to a thin slurry containing a lot of small quartz pebbles and a bunch of fine gold
2. strained and allowed whatever passed a (sorry, I can't find a number on it to be precise with mesh but it's blue, traps sand, and fits on a 5 gallon bucket if that helps ID it) fine sieve to settle out, then pouring off
**At this stage I took a sample from 15 lbs of a uniform powder I recovered from steps 1&2 which tested very consistently both as a powder and a bead -- but was determined to be out of the refiner's wheelhouse in that form.
"Enough Au content by far, but it would have to be melted into a solid." Unfortunately, the combination of my gravely limited grasp of smelting/flux/what-the-heck-I'm-even-doing and even more limited propane melting furnace has -- you guessed it-- limited my ability to make the jump from concentrate to metallic gold with that many impurities present. In an effort to avoid doing an AR process, (time constraints but also...I'm leery of turning gold I can see into gold I can't in a process I've done successfully before -- but I suspect mainly from luck) I scoured the forums for anything relevant. Did those things. I arrived at a powder that appears to meet all the physical criteria for a much higher purity Au by:
3. following the instructions for rinsing the mud in Hcl/Ammonia/water cycles found here on the forum + diluted sodium nitrate solution at one point for kicks
4. used stove and pyrex 9x13 to dry the mud in batches (though I do think it behaves more like cornstarch/water will when you try to manipulate it - which was cool, and surprised me)
4. Repeat.
There was a lot of free gold in the material, and any grit was easily snagged by the sieve, not to mention the filters; otherwise I would feel truly silly claiming these approx. values. That being said, I estimate I will end up with 35 or so lbs (18lbs currently processed with the additional cleaning steps) of a powder that, with a confirmed Au content of at least 55% should theoretically be easy to smelt for someone with the experience and equipment to do it properly. If you are that person and would like to speak about a really favorable trade for your services, please message me! Regarding the photos of the final result - I could not get a photo that showed the true color for some reason, but it is very much the pale cinnamon I have seen described here. Any glitter would be a residual Pyrex sliver from a near-catastrophic lesson in the limits of bakeware as labware that occasionally crop up and are removed. Thank you!
Andi
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