kjavanb123 said:
What temprature needed to incinerate? This waster incinerator unit I have tested produce 900c plus heat and oxygen and burns most of the smokes, so should I increase the heat to certain number?
Your temperature is accurate, but most likely there is no oxygen in between the boards (they stuck together) and therefore, they remain "black". When I incinerate chips I add them in small numbers just to cover the base of the vessel, when they are "cooked" and I add next layer. When vessel is half full, I empty it.
The problem in your list of procedures is ball mill. That is why assay shows low values. When you ball mill (half or fully) incinerated boards gold will be "lost" in ball mill, it would stick to the walls almost as plating.
When boards/ram are fully incinerated, you should be able to crash them with mortar and pestle very easy and than melt with excess borax and soda ash at around 1200-1300C.
You should be able to get single ball of mix metals. Scrape borax from crucible walls with rounded scraped while its hot and liquid. You probably will not be able to scrap all in a single pass. Once borax cools when you scrape, add more borax and some kryolite and put it back in the furnace. Let it melt and scrape again. Dissolve borax in dilute H2SO4, may take 1-2 days at room temperature, if you loose some metals in reaction with H2SO4, not so big of an issue, you final analysis will not be materially affected by much. You will recover small balls from borax. Remelt big ball with small balls. Now, you final alloy piece will be clean enough for chemical analysis.
You can either do chemical assay yourself or give the lab actual ball. Drilling the hole and giving a sample will be inaccurate as you have mix of metals with various consistency across the ball. The center will consist of mostly non precious metals except at the bottom. There is Pt in old 30pin ram sticks and absence of it in your lab report would mean it has been lost in the process.
Running 2Kg of old mixed ram (gold and tin plated) EDO (Extended Data Output) and SIMM (Single Inline Memory Module) yielded for me 1gr of gold and 0.05gr of Pt. That was my first ever try on chips incineration and I made many mistakes. I would have probably recovered more now.