Butcher,
I have another problem. I had at least 1, maybe 2 large pieces of Platinum Jewelry that tested to be Platinum. These were large brooches so there was a good bit of Platinum in these pieces. I think my wife added them in my last refine when she helped me clean up (one) day. When I decanted the first couple of times my decant solution was black, not greenish blue but black. I have read on the forum that Harold says that Platinum will dissolve in Nitric if the solution has silver in it. I know I had silver in the solution and I feel sure that my large Platinum pieces went into this last batch I ran. I have tried to get the silver to drop out of solution but I can't get the silver to drop? I know I have silver in it but it will not drop. I put a couple of drops of this black solution into a little HCL. I did see a little white cloud like appear this time. The first time I didn't see it, but I did the steps again and watched more closely. I believe I have dissolved my Platinum pieces in this black solution as well. I don't know how to go about recovering my Platinum out of these black decants that I feel my Platinum is in as well as silver? I have about 6 gallons of this blackish solution? Nothing that I have read addresses this particular circumstance? Can you give me any help with this?
Thanks Butcher,
Oneal
I have another problem. I had at least 1, maybe 2 large pieces of Platinum Jewelry that tested to be Platinum. These were large brooches so there was a good bit of Platinum in these pieces. I think my wife added them in my last refine when she helped me clean up (one) day. When I decanted the first couple of times my decant solution was black, not greenish blue but black. I have read on the forum that Harold says that Platinum will dissolve in Nitric if the solution has silver in it. I know I had silver in the solution and I feel sure that my large Platinum pieces went into this last batch I ran. I have tried to get the silver to drop out of solution but I can't get the silver to drop? I know I have silver in it but it will not drop. I put a couple of drops of this black solution into a little HCL. I did see a little white cloud like appear this time. The first time I didn't see it, but I did the steps again and watched more closely. I believe I have dissolved my Platinum pieces in this black solution as well. I don't know how to go about recovering my Platinum out of these black decants that I feel my Platinum is in as well as silver? I have about 6 gallons of this blackish solution? Nothing that I have read addresses this particular circumstance? Can you give me any help with this?
Thanks Butcher,
Oneal