Sodium Bromate

[kadriver]

Looking for a small quantity (100 grams or so) of sodium bromate for some experiments.

Can anyone suggest some sources - GFS Chemical (where I buy my acid) does not carry it.

kadriver

 

[Lou]

It can be easily made from sodium bromide at the pool supply.

http://www.sciencemadness.org/talk/viewthread.php?tid=21392

 

[kadriver]

Cool - thank you

 

[Lou]

If you can't get some maybe we can ship orm-d to you.

Do you want to try the Gilchrist hydrolysis? I can send some things for you if you promise to make a video and follow the procedure.

 

[kadriver]

Agreed! I will do as you requested, just let me know what you would like to do.

 

[Lou]

Cool. I can't upload attachments any more to the forum unfortunately (thank you Maiahost d'oh as they've banned my whole ISP) so it's great that you can do this.

Do you need crude Pt too? I figure you don't have indicator...

 

[rusty]

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[butcher]

Seems like the more security we get the more freedom we lose.

 

[kadriver]

Cool. I can't upload attachments any more to the forum unfortunately (thank you Maiahost d'oh as they've banned my whole ISP) so it's great that you can do this.

Do you need crude Pt too? I figure you don't have indicator...

Lou, I have Pt indicator solutions (100mg/100ml) if that is what you are refering to.

What I don't have is bromcresol purple, will I need that?

 

[kadriver]

Seems like the more security we get the more freedom we lose.

I agree butcher, it seems to come with the territory.

 

[Lou]

I do have some. I can also send you some 98% Pt contaminated with Rh and Ir that we usually do here.

Shoot me a PM with your contact and I'll give you a phone call.

 

[kadriver]

I found this video on Youtube that describes a method for producing sodium bromate.

[youtube]http://www.youtube.com/watch?v=PojvwUcMK4E[/youtube]

Any comments? Does this method look like it will work as described?

Thank you - kadriver

 

[Irons2]

It can be easily made from sodium bromide at the pool supply.

http://www.sciencemadness.org/talk/viewthread.php?tid=21392

Why can't one use Bromine instead?