Geo
Well-known member
Hydrated tin oxide (metastannic acid) can be removed completely in a short period of time.
First, add hydroxide to convert the tin hydrate to tin oxide. Very important, rinse well and dry the mass. Do not over heat or burn the salt. Dry on low heat. Once the salt is dry, add it to a beaker and add acetic acid. The tin oxide will dissolve instantly creating tin acetate. Any foils or solids should be rinsed well before processing further. The process only works if the salt is dry. It will not work on wet material.
I have used ammonia after drying the salts and it dissolves the salt but then you have to neutralize the solution.
First, add hydroxide to convert the tin hydrate to tin oxide. Very important, rinse well and dry the mass. Do not over heat or burn the salt. Dry on low heat. Once the salt is dry, add it to a beaker and add acetic acid. The tin oxide will dissolve instantly creating tin acetate. Any foils or solids should be rinsed well before processing further. The process only works if the salt is dry. It will not work on wet material.
I have used ammonia after drying the salts and it dissolves the salt but then you have to neutralize the solution.