mike6
Well-known member
Gentlemen.
First, let me express my gratitude for this forum, and to the members, without whom, my understanding of precious metal refining would not be augmented on a daily basis.
As this is my first post, kindly bear with me if I seem laborious in my question. I wish to get a meaningful answer first time round (without getting anyone's back up), and as such, feel that, the more information I give, the more concise the answer will be.
I have duplicated the silver cell as presented by "Palladium", and am achieving excellent results.
I refine .925 silver (coin and jewelry), .800 silver (coin), and .500 silver (coin). Step 1 of the process requires the dissolution of the raw stock, with nitric acid and distilled water. I use 70% nitric in the following ratios:
1).925- 1,45ml/g nitric, and an equal volume of water.
2).800-1,53ml/g nitric, and an equal volume of water.
3).500- 2,00ml/g nitric, and an equal volume of water.
Presently, I process each purity grade individually, as in my ignorance, I am afraid of messing up a tried and tested method. Logistically, as my batches are getting larger, I find more and more plastic containers, of different volumes, breeding uncontrollably!
Is the following hypothetical solution possible?
1kg of raw .925 would require 2900ml of dissolution liquid.
1kg of raw .800 would require 3060ml of dissolution liquid.
1kg of raw .500 would require 4000ml of dissolution liquid.
This is a total of 9960ml of liquid, technically, in the correct weight/volume ratio.
My question is thus, will I cause down-stream process problems, specifically during the cementation phase if I mix 3x 1kg batches, of differing purities (as specified above) into a single reaction vessel, and dissolve with the hypothetical 9960ml of dissolution liquid?, will full dissolution of the raw material even take place?
Please help!
First, let me express my gratitude for this forum, and to the members, without whom, my understanding of precious metal refining would not be augmented on a daily basis.
As this is my first post, kindly bear with me if I seem laborious in my question. I wish to get a meaningful answer first time round (without getting anyone's back up), and as such, feel that, the more information I give, the more concise the answer will be.
I have duplicated the silver cell as presented by "Palladium", and am achieving excellent results.
I refine .925 silver (coin and jewelry), .800 silver (coin), and .500 silver (coin). Step 1 of the process requires the dissolution of the raw stock, with nitric acid and distilled water. I use 70% nitric in the following ratios:
1).925- 1,45ml/g nitric, and an equal volume of water.
2).800-1,53ml/g nitric, and an equal volume of water.
3).500- 2,00ml/g nitric, and an equal volume of water.
Presently, I process each purity grade individually, as in my ignorance, I am afraid of messing up a tried and tested method. Logistically, as my batches are getting larger, I find more and more plastic containers, of different volumes, breeding uncontrollably!
Is the following hypothetical solution possible?
1kg of raw .925 would require 2900ml of dissolution liquid.
1kg of raw .800 would require 3060ml of dissolution liquid.
1kg of raw .500 would require 4000ml of dissolution liquid.
This is a total of 9960ml of liquid, technically, in the correct weight/volume ratio.
My question is thus, will I cause down-stream process problems, specifically during the cementation phase if I mix 3x 1kg batches, of differing purities (as specified above) into a single reaction vessel, and dissolve with the hypothetical 9960ml of dissolution liquid?, will full dissolution of the raw material even take place?
Please help!