Monkey-boy
Member
- Joined
- Jul 6, 2012
- Messages
- 7
@ jim
Yes sorry it was HCI I used
Yes sorry it was HCI I used
butcher said:That is the advice I would give "Go read nucklehead", it is the best way to learn. :lol:
oh never mindlazersteve said:Pete,
Check out the Guided Tour below and all links therein for details on processes and what they are used for as well as many other required reads.
Steve
goldpete said:oh never mindlazersteve said:Pete,
Check out the Guided Tour below and all links therein for details on processes and what they are used for as well as many other required reads.
Steve
i did say yesterday that i found the guided tour confusing ,
ill just wait till someone else asks the same questions and ill get my answer then
goldpete said:my daughter who is a hair dresser can get peroxide that is 12% which is a higher percentage than ive seen mentioned on this post so far .
will this be ok and how do i use AP ?
butcher said:Monkey-boy,
Assuming your trying the copper chloride leach, HCl, and dilute peroxide, and these are the reagents you used, except your peroxide was stronger 9%, you added a lot of oxygen to the mix which can attack the gold, as well as the copper, putting both metals into solution,
you could have diluted the peroxide with water, used less and used air as the primary oxidizer from a small fish tank air pump
goldpete said:do i still soak my material in nitric first , or is that what AP is for ?
goldpete said:from what i can figure out , AP is used prior to using AR
goldpete said:is AP used instead of AR
goldpete said:oh never mind
i did say yesterday that i found the guided tour confusing ,
ill just wait till someone else asks the same questions and ill get my answer then
awesome , so does that mean if AP is a recovery process ...... then i should use hcl/cl and then filter , wash and then use AP ?martyn111 said:goldpete said:my daughter who is a hair dresser can get peroxide that is 12% which is a higher percentage than ive seen mentioned on this post so far .
will this be ok and how do i use AP ?
As long as the peroxide that your daughter can get looks like water (not the cream type of peroxide) then you can use it, may supply is from a hairdresser, 12% like you are talking about, works fine.
Please see the quote from Butcher earlier in this thread.
butcher said:Monkey-boy,
Assuming your trying the copper chloride leach, HCl, and dilute peroxide, and these are the reagents you used, except your peroxide was stronger 9%, you added a lot of oxygen to the mix which can attack the gold, as well as the copper, putting both metals into solution,
you could have diluted the peroxide with water, used less and used air as the primary oxidizer from a small fish tank air pump
goldpete said:do i still soak my material in nitric first , or is that what AP is for ?
Better not to soak in nitric just in case there is solder present, tin in nitric is a nightmare, but you can remove it from the mix by pre soaking in HCl with added heat.
goldpete said:from what i can figure out , AP is used prior to using AR
With fingers and foils you can dissolve the gold with HCl /Cl which is an easier process for newcomers to use as the chlorine can easily be removed if you add too much, just heat, don't boil, and the excess chlorine will be liberated.
goldpete said:is AP used instead of AR
AP is a recovery process, releasing the gold from the substrate, AR is a refining process, dissolving the gold plus any remaining base metals and then selectively precipitating the gold from solution. Therefore AP isn't used instead of AR as the two processes are used to obtain different results in the overall processing of material.
oh ok thanks , so basically i use AP instead of a nitric soak ? , then i use hcl/cl as AR . then evaporate etcericrm said:no it mean you should use AP to free gold from contaminant(witch are the board,other base metal,plastic etc etc...)
hcl/cl is a refinning process (or cleaning your gold if you want) after that there is no need for another AP
edit you would use hcl/cl to dissolve your high purity gold 95%(just a number to show the idea),filter to remove big impurity like small plastic or board piece,or dirt,or silver and lead sulphate(when you will be there).
and than precipiate with smb to have clean gold powder
thats awesome , thankyou so much ,ericrm said:exactly :mrgreen:
except that hcl/cl doesnt need to be evaporate to a sirup ,just heated a little will drive the clorine out of solution
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