Copperas, Iron II sulfate, ferrous sulfate...degrades with time, temperature and humidity. It degrades into Iron III sulfate and Iron III oxide-hydroxide. Degradation is noted by a color change from pale green cristals to whiteish, yellowish, to brownish appearance. It should not be used. Get fresh greenish crystals. Prepare a solution by adding 50 grams of fresh Iron II sulfate in 100 ml distilled water for every 7.5 grams of expected gold. The solution will be pale green but cloudy. Heat gently, do not boil. Titrate the cloudy solution with hydochloric acid, drop by drop, until it clears. Filter the solution through a medium filter paper to remove anything isoluble such as free iron contaminants. It is now ready to use.